三氯化六氨合钴
![](https://math.21cnjy.com/MathMLToImage?mml=%3Cmath+xmlns%3D%22http%3A%2F%2Fwww.w3.org%2F1998%2FMath%2FMathML%22%3E%3Cmrow%3E%3Cmo%3E%5B%3C%2Fmo%3E%3Cmrow%3E%3Cmtext%3EC%3C%2Fmtext%3E%3Cmtext%3Eo%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmrow%3E%3Cmo%3E%28%3C%2Fmo%3E%3Cmrow%3E%3Cmtext%3EN%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmtext%3EH%3C%2Fmtext%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E3%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3C%2Fmrow%3E%3Cmo%3E%29%3C%2Fmo%3E%3C%2Fmrow%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E6%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3C%2Fmrow%3E%3Cmo%3E%5D%3C%2Fmo%3E%3C%2Fmrow%3E%3Cmtext%3EC%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmtext%3El%3C%2Fmtext%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E3%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3C%2Fmath%3E)
是合成其它一些Co(Ⅲ)配合物的原料,其在水中的溶解度随着温度的升高而增大。实验室用
![](https://math.21cnjy.com/MathMLToImage?mml=%3Cmath+xmlns%3D%22http%3A%2F%2Fwww.w3.org%2F1998%2FMath%2FMathML%22%3E%3Cmtext%3EC%3C%2Fmtext%3E%3Cmtext%3Eo%3C%2Fmtext%3E%3Cmtext%3EC%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmtext%3El%3C%2Fmtext%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E2%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3Cmo%3E%E2%8B%85%3C%2Fmo%3E%3Cmn%3E6%3C%2Fmn%3E%3Cmsub%3E%3Cmrow%3E%3Cmtext%3EH%3C%2Fmtext%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E2%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3Cmtext%3EO%3C%2Fmtext%3E%3C%2Fmath%3E)
晶体制备
![](https://math.21cnjy.com/MathMLToImage?mml=%3Cmath+xmlns%3D%22http%3A%2F%2Fwww.w3.org%2F1998%2FMath%2FMathML%22%3E%3Cmrow%3E%3Cmo%3E%5B%3C%2Fmo%3E%3Cmrow%3E%3Cmtext%3EC%3C%2Fmtext%3E%3Cmtext%3Eo%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmrow%3E%3Cmo%3E%28%3C%2Fmo%3E%3Cmrow%3E%3Cmtext%3EN%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmtext%3EH%3C%2Fmtext%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E3%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3C%2Fmrow%3E%3Cmo%3E%29%3C%2Fmo%3E%3C%2Fmrow%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E6%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3C%2Fmrow%3E%3Cmo%3E%5D%3C%2Fmo%3E%3C%2Fmrow%3E%3Cmtext%3EC%3C%2Fmtext%3E%3Cmsub%3E%3Cmrow%3E%3Cmtext%3El%3C%2Fmtext%3E%3C%2Fmrow%3E%3Cmrow%3E%3Cmn%3E3%3C%2Fmn%3E%3C%2Fmrow%3E%3C%2Fmsub%3E%3C%2Fmath%3E)
的实验步骤如下:
i.在锥形瓶中,将
溶于水中,加热至沸,加入研细的
晶体,溶解得到混合溶液;
ii.将上述混合液倒入三颈烧瓶中,加入活性炭。冷却,利用如图装置先加入浓氨水,再逐滴加入5%
溶液,水浴加热至50~60℃,保持20min;
![](http://tikupic.21cnjy.com/2023/04/13/5d/03/5d03ec658b6140a61eaac7a47d6d96a1_297x247.png)
iii.然后用冰浴冷却至0℃左右,吸滤,把沉淀溶于50mL沸水中,经操作X后,慢慢加入浓盐酸于滤液中,即有大量橙黄色晶体(
,
)析出;
iv.用冰浴冷却后吸滤,晶体以冷的盐酸洗涤,再用少许乙醇洗涤,吸干。回答下列问题: